GCMS analysis report for sample AE01037, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1102\1037.D Vial: 25 Acq On : 12 Feb 2002 9:32 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 2-Ethylacrolein Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.94 0.28 ug/1 25168 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Ethylacrolein 84 C5H80 000922-63-4 72 2 2-Pentenal, (E)- 84 C5H80 001576-87-0 64 3 2H-Pyran, 3,4-dihydro- 84 C5H8O 000110-87-2 56 4 2-Pentyn-l-ol 84 C5H80 006261-22-9 45

55 /Scalin 207 (6.944 min): 1037.D (-) C2) 2 5000

FG 1 ’ T' ' ' ' I 35 , 44 44 . 69 * 6.60 6.80 7.00 85.54% 7.20 TT-p-rT-ry-rr-r-rp- - ! m/z 3 9.05 11/2 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abu #551: 2-Ethylacrolen 55 84

5000 39 AyA । , AA ■ ' i ' ' ■ ■ i i 6.60 6.80 7.00 7.20 27 m/ z 55.0.0 73.98% 44 51 TBU00‘1‘ . 65 ■ । > ■ ■ ■ । ■ T mV > 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundarce 55 A AMA I ‘ ‘‘ f > I 27 6.60 6.80 7.00 7.20 39 84 5000 i m/ z 41.05 73.85%

51 66 69 ‘ A‘I‘‘‘II**‘II*‘‘‘I‘‘‘‘GIS‘SI‘ ‘SI‘‘*‘I‘‘SSI*AVSGVIIIIIUSIIIII‘I-SIAI‘I‘III mV- > 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 AbJ no #62716:2H-Pyran, 3,4-dihydro- 55 MAAAl 6.60 6.80 7.00 7.20 T’T

27 ' m/z 82.95.... 46.57% 5000- 84 39

m/-o FTnn 1 ■1' i ■' '' i' ■ ■ i ■ ■ ■ ■ । • 20 25 30 35 40 45 -9 50 - 69 111 ' ' ' i'' 11 । ' । । I । 11' I 55 60 65 70 75 80 85 90 6.60 6.80 ■ ।■ 1 1 i 1 1 ' • । 7.00 7.20

1037.D GCMS0208.M Tue Feb 19 10:32:03 2002 Page 1

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