GCMS analysis results for sample AE00838, Feb 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 5 0: Inst : Instrumen Mise : Ja 1.00 MS Integration

Quant Method : Title : DeyJAm ve Library : ************* ****** Peak Number 1 ank 6 t C R.T. Est( R.T.

36.29 1.: 34.42

Hit# of 5 Qual 1 Cholestan 00-08-5 43 2 Cholestan 00-08-5 43 3 Cholestan-3-one, (5 .ela. , 01-53-6 42 4 5.alpha.-Cholestan-3-one $$ Choi... 386 C27H460 000566-88-1 38 Abundance Scan 2883 (36.289 min): 00831 .D (-) m/z 95.10 100.00% 55 95 231 161 386 79 123 5000 213

145 316 189 353 36.00 36.20 36.40 36.60 01 ■ ■ t ■ ■1' i " " i " " i i ■ ■ ■' i' " r i m/z 55.10 99.06% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #324507: Cholestan-3-one 231

386 5000 95 36.00 36.20 36.40 36.60 123 m/z 43.10 80.28% 163

0 " r " 11 “ 1' i1" ■ i' T’i 247 ' i11" i I' ’ " I' " 11 363 111111"'11" " n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #324508: Cholestan-3-one $$ 3-Oxocholestane 231 386

36.00 36.20 36.40 36.60 5000 m/z 107.10 80 06%

95 124 163

m/z-> ...... 114. 247 275 0 h । . n-q n । । i . i'. । ‘ ‘111 ‘ ‘I‘ TT—nun—TTT 11111'" 1111" 11" " i " " i11 ‘11' 11 m 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 368

Abundance #324567: Cholestan-3-one, (5.beta.)- . PPPAA , ! r | , Mr PAA 43 36.00 36.20 36.40 36.60 m/z 231.2077.68%

5000 231 386

HHH .. 1.. ... 316... 368 1 161 0 TTTUITu‘nT"TTTTTTEECTET‘T‘TENITTTTTTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 36.00 36.20 36.40 36.60

30831.D SCAN508.M Fri Feb 01 09:18:44 2002 Page 15

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