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GCMS results for sample AE00699, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00699 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000052001–000052016

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C : \MSDCHEM\1\5973N\02JAN16\00699 . D Vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 16 14:05:05 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1122891 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4710465 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2474159 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 4146871 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3630816 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2619126 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 338093 5.16 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.20%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 10907 0.23 ug/L # 10 20) Dimethylphthalate 18.34 163 404818 2.48 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 312420 9.80 ug/L # 17 35) Di-n-butylphthalate 24.85 149 10526 0.04 ug/L i 76 41) Benzo(a)anthracene 30.49 228 8058 0.04 ug/L 4 49 42) Bis(2-ethylhexyl)phthalate 31.11 149 5187 0.58 ug/L i 44 43) Chrysene 30.4'9 228 8058 0.04 ug/L i 46 48) Benzo(a)pyrene 34.42 252 8272 0.05 ug/L i 1

(#) = qualifier out of range (m) = manual integration 00699.D SCAN508.M Wed Jan 16 14:05:06 2002 Page 1

NYC-WTC_000052003

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NYC-WTC_000052003Source: NYC Law Department, mirrored locally

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