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GCMS results for sample AE00740, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00740 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051984–000052000

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data,File : C:\MSDCHEM\1\5973N\O2JAN16\00740.D Vial: 8 Acq Ori : 16 Jan 2002 8:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 17 08:12:26 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCANS08

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1389218 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 5850158 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 3014016 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4981101 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4681700 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3654809 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 453379 5.76 ug/L 0.00 Spiked Amount 5.000 Recovery = 115.20% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 12187 0.21 ug/L # 11 20) Dimethylphthalate 18.34 163 492196 2.47 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 378137 9.74 ug/L # 17 35) Di-n-butylphthalate 24.85 149 30063 0.09 ug/L 98 41) Benzo(a)anthracene 30.50 228 17195 0.06 ug/L # 52 42) Bis(2-ethylhexyl)phthalate 31.11 149 116339 1.05 ug/L 94 43) Chrysene 30.50 228 17195 0.06 ug/L # 49 48) Benzo(a)pyrene 34.42 252 11757 0.05 ug/L # 1

(#) = qualifier out of range (m) = manual integration 00740.D SCAN508.M Thu Jan 17 08:12:27 2002 Page 1

NYC-WTC_000051986

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NYC-WTC_000051986Source: NYC Law Department, mirrored locally

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