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GCMS results for sample AE00315, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051380–000051393

Folder label: “GCMS X 1/8/02 A 1/11/02”

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 08:47:06 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1284670 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5420712 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2891681 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4907269 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4261457 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3083480 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 315360 4.07 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.40% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.61 74 7109 013 ug/L + 13 20) Dimethylphthalate 18.34 163 460628 2.41 ug/L t 55 21) 2,6-Dinitrotoluene 18.34 165 366063 9.83 ug/L i 17 35) Di-n-butylphthalate 24.85 149 22535 0.07 ug/L 97 41) Benzo(a)anthracene 30.50 228 11135 0.04 ug/L # 70 42) Bis(2-ethylhexyl)phthalate 31.11 149 10069 0.60 ug/L 89 43) Chrysene 30.50 228 11135 0.04 ugXL # 67 48) Benzo(a)pyrene 34.42 252 11185 0.06 ug/L # 1

(#) = qualifier out of range (m) = manual integration 00315.D SCAN508.M Tue Jan 15 08:47:07 2002 Page 1

NYC-WTC_000051382

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NYC-WTC_000051382Source: NYC Law Department, mirrored locally

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