GCMS results for sample AE00321, Jan 24 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN11\00321.D Vial: 2 Acq On : 11 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Misc : January 11, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 14 10:32:30 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1235098 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5215618 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 2673652 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.65 188 4423036 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 3969351 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3052128 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 295184 4.22 ug/L 0.00 Spiked Amount 5.000 Recovery = 84.40%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.61 74 12658 024 ug/L # 13 20) Dimethylphthalate 18.34 163 432247 2.45 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 344263 10.00 ug/L + 16 35) Di-n-butylphthalate 24.85 149 27414 0.10 ug/L 97 41) Benzo(a)anthracene 30.50 228 9415 0.04 ug/L # 76 42) Bis(2-ethylhexyl)phthalate 31.11 149 20147 0.65 ug/L 96 43) Chrysene 30.50 228 9415 0.04 ug/L + 73 48) Benzo(a)pyrene 34.42 252 10460 0.05 ug/L + 1

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(#) = qualifier out of range (m) = manual integration 00321.D SCAN508.M Mon Jan 14 10:32:31 2002 Page 1

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