GCMS results for sample AE00329, Jan 24 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN11\00329.D Vial: 3 Acq On : 11 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 14 10:32:31 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1080871 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4527529 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2421299 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.65 188 4210523 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 3815201 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2849235 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 282411 4.24 ug/L 0.00 Spiked Amount 5.000 Recovery = 84.80%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 9888 0.21 ug/L # 12 20) Dimethylphthalate 18.34 163 389092 2.43 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 309632 9.93 ug/L # 17 35) Di-n-butylphthalate 24.85 149 20231 0.07 ug/L 96 41) Benzo(a)anthracene 30.50 228 13039 0.06 ug/L # 74 42) Bis(2-ethylhexyl )phthalate 31.11 149 21550 0 .66 ug/L 88 43) Chrysene 30.50 228 10101 0.05 ug/L # 72 48) Benzo(a)pyrene 34.42 252 11773 0.06 ug/L + 1

(#) = qualifier out of range (m) = manual integration 00329.D SCAN508.M Mon Jan 14 10:32:32 2002 Page 1

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