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GCMS results for sample AE00704, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00704 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051914–000051929

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051918
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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN16\00704.D Vial: 4 - Acq On : 16 Jan 2002 5:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.476 7 9 13 rVB 29332 42154 0.33% 0.060% 2 3.602 17 20 25 rVB 29610 48358 0.38% 0.068% 3 4.835 123 128 139 rVB5 20100 75353 0.59% 0.106% 4 5.006 139 143 149 rVB 20833 41944 0.33% 0.059% 5 5.885 215 220 227 rBV 693852 1386796 10.93% 1.959%

6 7.438 353 356 367 rBV 57467 150118 1.18% 0.212% 7 8.237 421 426 441 rBV2 28011 72142 0.57% 0.102% 8 9.710 551 555 561 rBV 3617623 7072115 55.72% 9.992% 9 10.098 585 589 593 rBV2 48670 90650 0.71% 0.128% 10 13.192 855 860 865 rBV 5491773 10265335 80.88% 14.504%

11 18.341 1305 1311 1315 rBV 5837470 11544974 90.96% 16.312% 12 19.962 1447 1453 1461 rVB4 6606- 30597 0.24% 0.043% 13 22.280 1653 1656 1661 rW2 50799 88294 0.70% 0.125% 14 22.645 1681 1688 1693 rBV2 5518615 12692312 100.00% 17.933% 15 22.771 1695 1699 1713 rVB 69568 205634 1.62% 0.291%

16 24.849 1875 1881 1887 rBV 9986 32747 0.26% 0.046% 17 27.726 2129 2133 2137 rBV 1048683 1882596 14.83% 2.660% 18 30.489 2369 2375 2381 rBV2 4782874 11865594 93.49% 16.765% 19 31.105 2425 2429 2463 rW 1358722 3382846 26.65% 4.780% 20 34.416 2713 2719 2749 rW 3804674 9803991 77.24% 13.852%

Sum of corrected areas: 70774550

)0704.D SCAN508.M Thu Jan 17 08:17:33 2002 Page 1

NYC-WTC_000051918

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NYC-WTC_000051918Source: NYC Law Department, mirrored locally

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