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GCMS analysis results for sample AE00247, Jan 2002

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Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050539–000050557

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document L‘

Data File : C:\MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 ' Acq On : 24 Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 19 20 25 rBV 36816 60811 0.41% 0.074% 2 4.629 101 110 113 rBV4 21162 45866 0.31% 0.056% 3 4.846 123 129 141 rBV2 24119 79107 0.53% 0.097% 4 5.006 141 143 151 rVB 31311 62717 0.42% 0.077% 5 5.885 217 220 239 rBV 954384 1969804 13.25% 2.403% 6 9.562 539 542 547 rW 15391 37524 0.25% 0.046% 7 9.641 547 549 551 rW 16845 32186 0.22% 0.039% 8 9.721 551 556 561 rW 4687503 9388660 63.15% 11.454% 9 9.858 561 568 577 rW 20307 80622 0.54% 0.098% 10 12.541 799 803 807 rVB 24389 38254 0.26% 0.047% 11 13.192 855 860 865 rBV 6508075 13314307 89.55% 16.243% 12 16.549 1151 1154 1159 rBV 17501. 32547 0.22% 0.040% 13 18.341 1305 1311 1317 rW 7258417 14270509 95.98% 17.410% 14 22.280 1653 1656 1661 rBV 51937 104684 0.70% 0.128% 15 22.645 1681 1688 1693 rBV2 6745270 14868133 100.00% 18.139% 16 22.771 1697 1699 1709 rVB 84029 200741 1.35% 0.245% 17 27.726 2129 2133 2139 rBV 864862 1534860 10.32% 1.872% 18 30.500 2369 2376 2381 rBV 5693456 13784132 92.71% 16.816% 19 31.105 2419 2429 2437 rBV4 14846 60286 0.41% 0.074% 20 34.416 2713 2719 2747 rBV 4372070 12003635 80.73% 14.644%

Sum of corrected areas: 81969385

J0247.D SCAN508.M Fri Jan 25 10:26:03 2002 Page 1

NYC-WTC_000050543

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