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GCMS analysis results for sample AE00027, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.

NYC-WTC_000050735–000050753

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document L‘

Data File : C:\MSDCHEM\1\5973N\02JAN25\00027.D Vial: 3 . Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Insttumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 7 10 17 rVB 22641 39469 0.28% 0.051% 2 3.602 17 20 25 rBV 40324 59635 0.42% 0.077% 3 3.910 45 47 51 rW 19702 34226 0.24% 0.044% 4 4.241 73 76 85 rW5 14467 41203 0.29% 0.053% 5 4.629 107 110 117 rVB2 19428 42776 0.30% 0.055% .

6 4.835 123 128 137 rBV2 28534 71887 0.51% 0.093% 7 5.006 141 143 147 rBV 22393 36614 0.26% 0.047% 8 5.885 215 220 229 rBV 786691 1502490 10.63% 1.947% . 9 9.550 537 541 547 rBV5 15444 39007 0.28% 0.051% 10 9.710 551 555 561 rW 4523876 8548485 60.50% 11.075%

11 9.847 565 567 577 rW 18970 63539 0.45% 0.082% 12 13.192 855 860 865 rBV 6270734 12186538 86.25% 15.789% 13 18.341 1305 1311 1315 rBV 6653237 13124058 92.89% 17.003% 14 22.280 1651 1656 1661 rBV 55102 103501 0.73% 0.134% 15 22.645 1681 1688 1693 rBV 6329127 14129248 100.00% 18.306%

16 22.771 1697 1699 1711 rVB 81604 202367 1.43% 0.262% 17 27.726 2127 2133 2139 rBV 946602 1655470 11.72% . 2.145% 18 30.500 2369 2376 2381 rBV 5494659 13449366 95.19% 17.425% 19 31.094 2423 2428 2445 rW5 11835 55700 0.39% 0.072% 20 34.416 2713 2719 2751 rBV 4243524 11799022 83.51% 15.287%

Sum of corrected areas: 77184601

30027.D SCAN508.M Mon Jan 28 09:49:28 2002 Page 1

NYC-WTC_000050739

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NYC-WTC_000050739Source: NYC Law Department, mirrored locally

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