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GCMS analysis results for sample AE00558, Jan 2002

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Laboratory report showing GCMS analysis results for sample AE00558 conducted on January 17, 2002.

NYC-WTC_000051714–000051726

Folder label: “GCMS X 1/9/02 A 1/15/02”

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NYC 9/11 Public Portal Document aepoIC (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN15\00558.D Vial: 2 Acq On : 15 Jan 2002 2:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:52 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 971717 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4089999 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 2129392 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 3556806 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3201403 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2277220 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 267092 4.75 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 7779 0.19 ug/L i 1 20) Dimethylphthalate 18.34 163 342350 2.43 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 270900 9.88 ug/L # 17 . 35) Di-n-butylphthalate 24.85 149 26689 0.12 ug/L 96 ) 41) Benzo(a)anthracene 30.49 228 7814 0.04 ug/L # 47 42) Bis(2-ethylhexyl)phthalate 31.11 149 86805 1.09 ug/L 87 43) Chrysene 30.49 228 7360 0.04 ug/L # 45 48) Benzo(a)pyrene 34.42 252 8028 0.05 ug/L + 1

+) = qualifier out of range (m) = manual integration )558.D SCAN508.M Tue Jan 15 15:51:53 2002 Page 1

NYC-WTC_000051716

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NYC-WTC_000051716Source: NYC Law Department, mirrored locally

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