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GCMS results for sample AE00702, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051895–000051913

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 . Acq On : 16 Jan 2002 3 :57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 17 08:12:19 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1296603 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5475389 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2925848- 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.65 188 4854324 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4217566 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3196454 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 424325 5.53 ug/L 0.00 Spiked Amount 5.000 Recovery = 110.60% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 12024 0.22 ug/L # 12 20) Dimethylphthalate 18.34 163 465506 2.41 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 369373 9.80 ug/L # 17 35) Di-n-butylphthalate 24.85 149 29426 0.09 ug/L 95 41) Benzo(a)anthracene 30.50 228 8605 0.03 ug/L # 46 42) Bis(2-ethylhexyl)phthalate 31.11 149 120393 1.12 ug/L 93 43) Chrysene 30.50 228 8605 0.03 ug/L # 44 48) Benzo(a)pyrene 34.42 252 9848 0.05 ug/L # 1

(#) = qualifier out of range (m) = manual integration 00702.D SCAN508.M Thu Jan 17 08:12:20 2002 Page 1

NYC-WTC_000051897

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NYC-WTC_000051897Source: NYC Law Department, mirrored locally

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