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GCMS results for sample AE00701, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051877–000051894

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN16\00701.D Vial: 1 . Acq On : 16 Jan 2002 3:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 17 08:12:18 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1093872 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 4622818 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2421298. 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.63 188 4100961 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3715484 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2786372 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 362952 5.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 112.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 8567 0.18 ug/L # 17 20) Dimethylphthalate 18.34 163 390914 2.44 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 304348 9.76 ug/L # 17 35) Di-n-butylphthalate 24.85 149 39705 0.15 ug/L 97 41) Benzo(a)anthracene 30.50 228 8685 0.04 ug/L # 56 42) Bis(2-ethylhexyl)phthalate 31.11 149 86763 1.02 ug/L 98 43) Chrysene 30.50 228 8684 0.04 ug/L # 53 48) Benzo(a)pyrene 34.42 252 10162 0.06 ug/L # 1

(#) = qualifier out of range (m) = manual integration 00701.D SCAN508.M Thu Jan 17 08:12:19 2002 Page 1

NYC-WTC_000051879

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NYC-WTC_000051879Source: NYC Law Department, mirrored locally

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