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GCMS analysis results for sample AE00365, Jan 2002

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Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.

NYC-WTC_000051685–000051696

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00365.D Vial: 3 Acq On : 15 Jan 2002 11:52 am Operator: ■ Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:48 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 965355 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4083466 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 2113368 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 3608493 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3137970 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2187136 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 280254 4.91 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.20% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 7170 0.17 ug/L # 15 20) Dimethylphthalate 18.34 163 337839 2.42 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 273192 10.04 ug/L # 17 35) Di-n-butylphthalate 24.85 149 58644 0.25 ug/L 99 41) Benzo(a)anthracene 30.49 228 9059 0.05 ug/L # 52 42) Bis(2-ethylhexyl)phthalate 31.11 149 5097 0.58 ug/L # 53 43) Chrysene 30.49 228 9059 0.05 ug/L + 50 48) Benzo(a)pyrene 34.42 252 8593 0.06 ug/L + 1

(#) = qualifier out of range (m) = manual integration 00365.D SCAN508.M Tue Jan 15 15:51:48 2002 Page 1

NYC-WTC_000051687

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NYC-WTC_000051687Source: NYC Law Department, mirrored locally

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