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GCMS analysis results for sample AE00470, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.

NYC-WTC_000051697–000051713

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN15\00470.D Vial: 4 Acq On : 15 Jan 2002 12:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:49 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1141364 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4854299 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2566552 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4241704 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 3808659 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2740294 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 328864 4.90 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 9478 0.19 ug/L # 13 20) Dimethylphthalate 18.34 163 407628 2.40 ug/L + 56 21) 2,6-Dinitrotoluene 18.34 165 326985 9.89 ug/L # 17 35) Di-n-butylphthalate 24.85 149 48487 0.18 ug/L 94 41) Benzo(a)anthracene 30.49 228 9452 0.04 ug/L # 52 43) Chrysene 30.49 228 9452 0.04 ug/L + 49 48) Benzo(a)pyrene 34.42 252 9551 0.05 ug/L f 1

(#) = qualifier out of range (m) = manual integration 00470.D SCAN508.M Tue Jan 15 15:51:50 2002 Page 1

NYC-WTC_000051699

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NYC-WTC_000051699Source: NYC Law Department, mirrored locally

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