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GCMS results for sample AE00468, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051318–000051335

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051320
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN10\00468.D Vial: 5 Acq On : 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 11 10:18:54 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Last Update : Thu Jan 10 11:01:02 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1166614 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4874107 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2513226 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.63 188 4115686 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3701613 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2740235 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 298791 4.59 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.80% Target Compounds Qvalue 2) n-Nitroso-dimethylamine 3.60 74 8317 0.17 ug/L # 13 20) Dimethylphthalate 18.34 163 409112 2.46 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 325548 10.06 ug/L # 17 35) Di-n-butylphthalate 24.86 149 18625 0.07 ug/L 94 41) Benzo(a)anthracene 30.49 228 9223 0.04 ug/L # 54 42) Bis(2-ethylhexyl)phthalate 31.12 149 19153 0.65 ug/L 91 43) Chrysene 30.49 228 9223 0.04 ug/L # 51 48) Benzo(a)pyrene 34.42 252 9216 0.05 ug/L # 1

(#) = qualifier out of range (m) = manual integration 00468.D SCAN508.M Fri Jan 11 10:18:55 2002 Page 1

NYC-WTC_000051320

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NYC-WTC_000051320Source: NYC Law Department, mirrored locally

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