GCMS analysis results for sample AE00615, Feb 2002

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 ‘ Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 30 08:25:58 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1634446 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 6920965 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 3669340- 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.65 188 6105428 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 5275682 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3720825 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 419250 4.34 ug/L 0.00 Spiked Amount 5.000 Recovery = 86.80% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 581246 2.40 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 465428 9.85 ug/L # 17 35) Di-n-butylphthalate 24.85 149 102074 0.26 ug/L 100 42) Bis(2-ethylhexyl)phthalate 31.09 149 12372 0.60 ug/L 79

(#) = qualifier out of range (m) = manual integration 00615.D SCAN508 .M Wed Jan 30 08:25:59 2002 Page 1

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