GCMS analysis results for sample AE00615, Feb 2002

NYC 9/11 Public Portal Document

LLDLCLY >earcr compound Keporc

Data File : C:\MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Cyclopentanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.85 0.17 ug/L 77171 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanone 84 C5H8O 000120-92-3 25 2 5-Hexenal oxime 113 C6H11NO 057606-82-3 12 3 1-Hexene, 6-bromo- 162 C6H11Br 002695-47-8 10 4 1-Hexene, 6-bromo-_______________ 162 C6HllBr 002695-47-8 10 Abundance Scan 129 (4,846 min): 00615.D (-) m/z 83.95 100.00% 84 55 41 __ 5000

4.40 4.60 4.80 5.00 5.20 — m/z 55.10 59.36% ■ • ■ ■ ■ i1 ■ ■' i ■

n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3268: Cyclopentanone 55

5000 41 84 - 4.40 4.60 4.80 5.00> 5.20 A- 27 m/ z 41.10 52.39% - 18‘ i11'' i TT

.N N. ■ 111 ■1111 ’' i ■ i'1'' i1 1 1 r i'1111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #14234: 5-Hexenal oxime 41 55

440 4.60 4.80 5.00 5.20 5000 27 m/z 59.10 42.31%

11"101010011—001111TTTT 113 i ■ " 11 i'11 ■ i i111111 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance 41 55 #61497:1-Hexene, 6-bromo- moutipoet ............ A 4.40 4.60 4.80 500 5.20 m/z 39.10 39.68% 83 5000 27 67

TTTUtItnrT - 134 162 ' i1'1' i' " ' i 1'' i ■'1' i1 • ■' i1 " ' i1' ■ ■ i'1 " i'' '' i''1 ■ i ‘■ i' m/z— > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4.40 4.60 4.80 5.00 5.20

>0615.D SCAN508.M Wed Jan 30 09:02:20 2002 Page 6

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