GCMS analysis results for sample AE00555, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00555.D Vial: 1 Acq On : 29 Jan 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

3.48 0.10 ug/L 49263 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 39 4 Allyl mercaptan $$ CH2=CHCH2SH $... 74 C3H6S 000870-23-5 9 Abundance Scan 9 (3.477 min): 00555.D (-) m/ z 74.00 100.00% 74 82 5000

47 TIOBtgrr 3.50 3.60 3.70 3.80 3.90 TTTTTTIITPTITIT 38 II m/z 81.90 60.59% Tbit l ■ i ■ ■ ■ * i 1 ■ ■ ■ I • ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82

5000 4)0 3.50 3.60 3.70 3.80 3.90 47 m/z 83.90 41.59% 35

/z-> 12 ■ ' i1 ■ ■ 1 । ■ ' 1 ■ । ■ 10 20 30 +P■ 40 50 60 1 i ■ 1 1 ■ i 1 70 80 90 ---194— 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 7|4

3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 39.52% 47 35 - m/z-> 10 20 30 40 50 1 I 1 r 1 1 I '' 60 70 80 I- 90 ... 100 -199. 110 Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 35 m/z 47.00 21.19%

5000 82

47 1 ' | 1 ' ' 1 | I । l—r | 1 T’l’l'l "1 ' 1 l m/z—> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

3555.D SCAN508.M Wed Jan 30 09:01:51 2002 Page 3

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