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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02”

←Page 7 of 20→
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01141 .D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: : Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.50 0.13 ug/L 53929 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 4 Thietane (CAS) $$ Thiacyclobutan... 74 C3H6S 000287-27-4 37 Abundance Scan 11 (3.498 min): 01141 .D (-) m/z 74.00 100.00% 74

5000 82 47 3.50 3.60 3.70 3.80 3.90 ol । i । i . . IIp" . . ■ । 1 ' ■ ■ । 1 ‘ill 4TI m/Z 81.85 44.41% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 47 3.50 3.60 3.70 3.80 3.90 m/z 83.90 33.24% 35

iz-> ol ...... 10 20 ....30 , rIp 40 50 1 i ' ' 1 ' i ' 60 70 I TIl 80 1....... 90 1 " 109 - 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35 TI i ' ' 1 ‘ i ■ ■ ■ 1 i ■ ' ' ' i 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 31.41% 47

Of . i r ‘ ' i ' ' r ‘ i ' ' 1 — _________________ ' 1 I 1 1 1 1 I ' L TTid 1 ' i r 1 ■ 1 i ■ ' 1 ■ i ■ ' miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 3.50 3.60 3.70 3.80 3.90 m/z 47.00 22.84%

5000 47 35

/z-> 0 ...2 10 ........... 20 30 1 .!, 40 .. H........... - 11t l ■ i ■ ■ ■ ■ t ■ rr t r 50 60 70 80 1 90 100 110 108 M, ........ fl..../.. 3.50 3.60 3.70 3.80 3.90

01141.D HP022102.M Tue Feb 26 08:30:25 2002 Page 3

NYC-WTC_000003549

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NYC-WTC_000003549Source: NYC Law Department, mirrored locally

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