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GCMS results for sample AE00314, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051364–000051379

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051366
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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN14\00314 .D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 08:47:05 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1243589 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5281692 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2756804 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4556828 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 3977974 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3004618 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 317110 4.40 ug/L 0.00 Spiked Amount 5.000 Re co ery = 88.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.61 74 12161 0.23 ug/L # 17 20) Dimethylphthalate 18.34 163 444273 244 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 353744 9.96 ug/L # 17 35) Di-n-butylphthalate 24.85 149 26276 0.09 ug/L 88 41) Benzo(a)anthracene 30.49 228 9763 0.04 ug/L # 61 42) Bis(2-ethylhexyl)phthalate 31.11 149 6443 0.58 ug/L # 68 43) Chrysene 30.49 228 9763 0.04 ugXL # 58 4 8) Benzo(a)pyrene 34.42 252 10207 0.05 ug/L # 1

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(#) = qualifier out of range (m) = manual integration 00314.D SCAN508.M Tue Jan 15 08:47:06 2002 Page 1

NYC-WTC_000051366

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NYC-WTC_000051366Source: NYC Law Department, mirrored locally

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