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GCMS results for sample AE00471, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051301–000051317

Folder label: “GCMS X 1/8/02 A 1/10/02”

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Scanned page image, NYC-WTC_000051305
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LbC area Percent Keporc

Data File : C:\MSDCHEM\1\5973N\02JAN10\00471.D Vial: 6 Acq On 10 Jan 2002 6:57 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508 .M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rVB 31073 58535 0.55% 0.097% 2 4.629 101 110 125 rVB 17487 52684 0.49% 0.087% 3 4.846 125 129 139 rBV2 20023 57269 0.54% 0.094% 4 5.006 139 143 149 rVB 95940 164603 1.54% 0.271% 5 5.703 201 204 209 rW 57915 115149 1.08% 0.190%

6 5.885 217 220 243 rW 847730 1717170 16.05% 2.832% 7 9.710 551 555 561 rW 3295062 6550947 61.24% 10.803% 8 9.847 561 567 573 rW 20228 62305 0.58% 0.103% 9 13.192 855 860 865 rBV 4952536 9284551 86.79% 15.311% 10 18.341 1305 1311 1315 rBV 5139094 10038236 93.84% 16.554%

11 20.933 1535 1538 1543 rVB 29828 47013 0.44% 0.078% 12 22.280 1653 1656 1661 rBV2 40147 72698 0.68% 0.120% 13 22.634 1681 1687 1693 rBV2 4752475 10697467 100.00% 17.641% 14 22.771 1695 1699 1711 rVB 58043 152277 1.42% 0.251% 15 27.726 2129 2133 2139 rBV 738921 1276023 11.93% 2.104%

16 29.918 2319 2325 2331 rVB 54715 102192 0.96% 0.169% 17 30.489 2369 2375 2381 rBV2 4463560 10645719 99.52% 17.556% 18 30.660 2387 2390 2401 rVB 49215 143641 1.34% 0.237% 19 34.416 2713 2719 2753 rBV 3659985 9357442 87.47% 15.431% 20 35.661 2823 2828 2833 rW3 16817 42754 0.40% 0.071%

Sum of corrected areas: 60638675

)0471.D SCAN508.M Fri Jan 11 10:08:48 2002 Page 1

NYC-WTC_000051305

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NYC-WTC_000051305Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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