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GCMS analysis results for sample AD31637, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.

NYC-WTC_000049929–000049943

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000049933
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Keporc Data File : C:\MSDCHEM\1\5973N\02JAN17\31637.D Vial: 4 • Acq On : 17 Jan 2002 12:42 pm Operator: 'Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.476 7 9 15 rVB 30241 47823 0.41% 0.077% 2 3.602 15 20 25 rBV 38086 70084 0.60% 0.113% 3 4.241 71 76 83 rVB4 13531 38262 0.33% 0.062% 4 4.367 83 87 91 rBV2 20405 32854 0.28% 0.053% 5 4.618 107 109 125 rVB4 21717 53303 0.46% 0.086% 6 4.835 125 128 135 rBV3 26037 66044 0.57% 0.107% 7 5.006 141 143 149 rVB5 17787 28474 0.24% 0.046% 8 5.885 215 220 245 rBV 763765 1648276 14.15% 2.668% 9 9.710 551 555 561 rBV 3240413 6473013 55.55% 10.478% 10 13.192 855 860 865 rBV 4887233 9315889 79.95% 15.080% 11 18.341 1305 1311 1315 rBV 5377441 10534368 90.40% 17.052% 12 19.985 1443 1455 1459 rBV5 5460 27883 0.24% 0.045% 13 22.280 1651 1656 1661 rVB 43853 81654 0.70% 0.132% 14 22.645 1681 1688 1693 rBV2 5066036 11652699 100.00% 18.863% 15 22.771 1695 1699 1705 rVB 60375 135752 1.16% 0.220% 16 24.849 1877 1881 1891 rW 75112 137508 1.18% 0.223% 17 27.726 2129 2133 2139 rBV 924707 1632792 14.01% 2.643% 18 30.489 2369 2375 2381 rBV 4359276 10801980 92.70% 17.485% 19 31.094 2425 2428 2437 rW5 11390 34569 0.30% 0.056% 20 34.416 2713 2719 2753 rBV 3453901 8963748 76.92% 14.510%

Sum of corrected areas: 61776975

31637.D SCAN508.M Tue Jan 22 08:36:58 2002 Page 1

NYC-WTC_000049933

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NYC-WTC_000049933Source: NYC Law Department, mirrored locally

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