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GCMS blank analysis results for sample AE00167, Jan 2002

Machine-extracted title · confidence 100%

Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.

NYC-WTC_000050444–000050480

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050465
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NYC 9/11 Public Portal Document Lt area Percent KepOrC Data File : C:\MSDCHEM\1\5973N\02JAN25\0104B2.D Vial: 4 Acq On : 25 Jan 2002 12:39 pm Operator: Sample : lab blank 1/4; 2nd inj. Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 15 20 25 rBV 21792 31973 0.27% 0.053% 2 4.367 83 87 93 rVB 8445 17296 0.15% 0.029% 3 4.630 107 110 121 rW4 10279 25459 0.22% 0.042% 4 4.858 123 130 139 rW5 10641 37918 0.32% 0.063% 5 5.006 139 143 151 rVB3 10945 25150 0.22% 0.042% 6 5.897 217 221 245 rW 443169 1216096 10.40% 2.011% 7 9.413 527 529 535 rVB 10703 18578 0.16% 0.031% 8 9.710 551 555 563 rBV 3269343 6840825 58.52% 11.313% 9 12.541 799 803 807 rVB 13007 22119 0.19% 0.037% 10 13.192 855 860 865 rBV 5037187 9736652 83.29% 16.102%

11 13.375 873 876 883 rVB 9347 18200 0.16% 0.030% 12 16.549 1149 1154 1161 rVB2 8192- 18194 0.16% 0.030% 13 18.341 1305 1311 1315 rBV 5516032 10795399 92.34% 17.853% 14 22.280 1653 1656 1661 rBV2 35966 70550 0.60% 0.117% 15 22.634 1681 1687 1693 rBV2 5252461 11690441 100.00% 19.333%

16 22.771 1697 1699 1705 rVB 54553 104784 0.90% 0.173% 17 27.726 2129 2133 2139 rBV 524196 934580 7.99% 1.546% 18 30.489 2369 2375 2415 rBV2 4358645 10592388 90.61% 17.517% 19 34.416 2713 2719 2749 rBV 3101541 8253463 70.60% 13.649% 20 39.051 3121 3125 3131 rBV4 3723 18624 0.16% 0.031%

Sum of corrected areas: 60468689

1104B2.D SCAN508.M Fri Jan 25 13:22:48 2002 Page 1

NYC-WTC_000050465

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NYC-WTC_000050465Source: NYC Law Department, mirrored locally

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