GCMS analysis results for sample AD31672, Jan 28 2002

NYC 9/11 Public Portal Document LBC Area Percent KepOrC Data File : C:\MSDCHEM\l\5973N\02JAN17\31672.D Vial: 7 * Acq On : 17 Jan 2002 7:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rBV 34380 52169 0.45% 0.083% 2 3.990 51 54 59 rW 11845 25109 0.22% 0.040% 3 4.241 71 76 83 rBV4 30044 70054 0.61% 0.112% 4 4.367 83 87 91 rBV2 13361 26009 0.23% 0.042% 5 4.618 107 109 117 rVB 18060 39139 0.34% 0.062% 6 4.835 125 128 139 rBV3 27967 71081 0.62% 0.113% 7 5.885 217 220 247 rVB 707629 1492977 12.98% 2.383% 8 9.413 525 529 535 rBV3 11313 30731 0.27% 0.049% 9 9.710 551 555 561 rBV 3438188 6691739 58.18% 10.683% 10 12.747 815 821 831 rBV3 8505 33724 0.29% 0.054% 11 13.192 855 860 865 rBV 5065660 9581385 83.30% 15.296% 12 18.341 1305 1311 1315 rBV 5367348 10515269 91.42% 16.787% 13 22.280 1653 1656 1661 rVB 47876 86693 0.75% 0.138% 14 22.634 1681 1687 1693 rBV2 5106354 11502493 100.00% 18.363% 15 22.771 1695 1699 1711 TVB 66097 188124 1.64% 0.300% 16 24.849 1877 1881 1887 rBV 87749 163975 1.43% 0.262% 17 27.726 2129 2133 2139 rW 773062 1363624 11.86% 2.177% 18 29.690 2299 2305 2313 rVB5 6752 27713 0.24% 0.044% 19 30.489 2369 2375 2381 rBV2 4537835 11133118 96.79% 17.773% 20 34.416 2713 2719 2747 rBV 3722687 9545205 82.98% 15.238%

Sum of corrected areas: 62640331

31672.D SCAN508.M Tue Jan 22 08:37:29 2002 Page 1

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