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GCMS analysis results, sample AE10987, May 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AE10987 completed May 22, 2002, showing unknown compounds and surrogate recovery at 89%.

NYC-WTC_000024463–000024471

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024467
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LbC Area Percent Keporc

Data File : C:\MSDCHEM\1\DATA\020515\10987.D Vial: 17 Acq On : 16 May 2002 3:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.158 516 524 560 rBV 828320 1668946 37.61% 6.132% 2 11.375 1401 1412 1434 rBV 1236990 3153460 71.07% 11.586% 3 16.534 2275 2290 2307 rBV 1566321 3977174 89.63% 14.613% 4 24.460 3618 3639 3655 rBV 1501346 4145153 93.41% 15.230% 5 27.551 4142 4165 4179 rBV2 927652 2704784 60.95% 9.938%

6 31.717 4855 4874 4904 rBV2 1452.771 4437369 100.00% 16.304% 7 31.958 4907 4915 4923 rVB3 10866 31584 0.71% 0.116% 8 39.931 6259 6272 6295 rBV2 1897100 3842601 86.60% 14.118% 9 40.518 6363 6372 6403 rVB2 243773 589904 13.29% 2.167% 10 43.151 6808 6820 6853 rBV 1271956 2665847 60.08% 9.795%

Sum of corrected areas: 27216822

10987.D SCAN020507.M Thu May 16 09:24:39 2002 Page 1

NYC-WTC_000024467

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NYC-WTC_000024467Source: NYC Law Department, mirrored locally

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