GCMS blank results for sample AE00275, Jan 2002

NYC 9/11 Public Portal Document

blbrary Search Compound Report

Data File : C:\MSDCHEM\1\5973N\O2 JAN08\BLEX0107.D Vial: 1 • Acq On 8 J an 2002 4:18 pm Operator: Sample : blank - ext 1/7/02 Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 3-Buten-2-ol, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.14 ug/L 47223 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 59 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 53 3 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 38 4 Pentane, 2-bromo- (CAS) $$ 2-Bro... 150 C5HllBr 000107-81-3 36 Abundance Scan 143 (5.006 min): BLEX0107. D (-) m/z 71.00 100.00% 43 71

5000 55 59

39 84 4.60 —4.80A— 5.00 'I ""TTrrrrl > > 5.20 5.40 - ----- 01 ‘I’r T’T m/ z 43.10 93.13% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4084:3-Buten-2-ol, 2-methyl- 71 43

5000 59 LMD A 460 4.80 5.00 5.20 5.40 m/z 41.10 80.22% 27 53 V i 67 86

m/z-> OFTT 20 TTTTPTTTTI TIT -HH 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 —TTPTTHPT

Abundance #4085: 3-Buten-2-ol, 2-methyl- 71 43 -------A 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 50.84% 59 27 31 53 86 Of 111 ■'' ■ i' ‘ It ■11' ''' i'' +T l ’ > । ■ ■ ■ ■ । ■ 11 ■ ■ < । ■ • • ■ । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #9384:2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... ■ i 1 ■ ■ 1 i ■ ' ■ ' 1 1 1 1 1 1 ' 'I 1 '■ 71 460 4.80 5.00 5.20 5.40 43 m/z 55.00 39.91%

5000 27 31

37 m/z-> 0 ■ ■ i ■ ■ ■ ■ i1 "‘It " 1111111' 20 25 30 35 40 145. 50...... H

55 60 65 70 75 80 85 90 95 ।1111 ■'1 r ■1 r i ■ ■111 ■ ■ ■ ■ i

4.60 TT 4.80 ' ■ T' ' 1 1 I '■ ■ ■ i ' 1 5.00 5.20 5.40

BLEX0107.D SCAN508.M Wed Jan 09 15:08:05 2002 Page 5

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