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GCMS analysis results for sample AE00166, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.

NYC-WTC_000050683–000050701

Folder label: “GCMS X 1/4/02 A 2/4/02

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Scanned page image, NYC-WTC_000050700
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Data File : C: \MSDCHEM\1\5973N\02FEB04\00166 . D Vial: 5 • Acq On 4 Feb 2002 6:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.43 ug/L 428177 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm . CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 87 3 Phenanthrene-diO 188 C14D10 001517-22-2 64 4 Acridine-D9 188 C13D9N 000000-00-0 64 Abundance Scan 1699 (22.771 min): 00166. D (-) m/z 188.10 100.00% 188

5000

94 80 1A6 158 —184 22.40 22.60 22.80 23.00 23.20 m/z—> 42 52 66 102 O' —Hpt —H TTthe 122 132 — f 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.10 21.64% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 80.10 15.95% 158 66 Of TTTIWWTTIWWTTPTTITTT TTTTf mmmmPmmpmpm miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.15 14.75%

80 94 160 Ji 66 Op “ I ’ ‘’ 1 ‘ ■1 * i “ ’1111 ■ 30 ---1 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 —। । i । । । (। n > i । > । t । । । [• i 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 12.98% 5000

94 80 160 66 O mmmmmpmhpot -419 ' “ ‘ JI “ I “ “ I ‘'111" 11 “ 1111 iz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -- 22.40 22.60 22.80 23.00 23.20

)0166.D SCAN508.M Tue Feb 05 09:47:41 2002 Page 14

NYC-WTC_000050700

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NYC-WTC_000050700Source: NYC Law Department, mirrored locally

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