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GCMS analysis results for sample AE00166, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.

NYC-WTC_000050683–000050701

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document **.Z

Data File : C: \MSDCHEM\1\5973N\02FEB04\00166.D Vial: 5 • Acq On : 4 Feb 2002 6:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 10 1-(4-Chlorophenyl)-1-propanol Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.07 ug/L 64916 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-(4-Chlorophenyl )-1-propanol 170 C9H11C1O 000000-00-0 38 2 4-methoxymethyl-2-methylthiopyri... 170 C7H10N2OS 123061-70-1 38 3 2,5-Cyclohexadiene- 1,4-dione, 2,... 140 C6H404 000615-94-1 25 4 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 035069-70-6 25 Abundance Scan 1154 (16.549 min): 00166. D (-) m/z 140.20 100.00% 140

5000 43 56 71 89 122 172 16.20 16.40 16.60 16.80 ‘ ‘ miz-> Oh —mmmmP II.................. I...... ’ ’I’ ■1' ■ i ■ • ■ ■ i ■ ■ ■' । 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ■11 1t18 i ■ **’1***’}’* m/z 71.10 37.98% Abundance #72984: 1-(4-Chlorophenyl)-1 -propanol 140

5000 16.20 16.40 16.60 16.80..... 113 m/z 56.10 35.43% 170 Oh 111' • • • i ■ ■1 ‘ i1 i1 • “ i ■ ■ • ■ i ■1 ■ ‘ i ■ ■111 1 11 r 11111 l. ■■i■1 ■ ■ i ■ ■1 • I11 ■ ■ i' niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #72568:4-methoxymethyl-2-methylthiopyrimidine $$ Pyrimidi... 140

16.20 16.40 16.60 16.80 5000 m/z 89.00 32.86% 45

miz-> Oh ■ ■ i ■ ■ ■ ■ i ■ 30 40 50 i111' FT1 111* i k f 4 EE 170 125 11 > 111 j 11 ■ 111 60 70 80 90 100 110 120 130 140 150 160 170 180 L

Abundance #35124:2,5-CycIohexadiene-1,4-dione, 2,5-dihydroxy- 140 16.20 16.40 16.60 16.80 " ' ‘ 42 69 m/z 122.10 32.63%

5000 53 84 94 112

Of ’’11 1 ■ i1 ■ ■ ■ i1 • 1.... 1111 ■ •>I I I I Immp 1*............ I I ■ ■111"' i ■11 ■ i ‘ _। ■ • • i • ' ■ ■ i ■ ■ • 1 i 1 ■ • ■ i ‘ ■ i ' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 16.20 16.40 16.60 16.80

50166.D SCAN508.M Tue Feb 05 09:47:40 2002 Page 12

NYC-WTC_000050698

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NYC-WTC_000050698Source: NYC Law Department, mirrored locally

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