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GCMS analysis results for sample AE00166, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.

NYC-WTC_000050683–000050701

Folder label: “GCMS X 1/4/02 A 2/4/02

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Scanned page image, NYC-WTC_000050697
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NYC 9/11 Public Portal Document uoLa y oeaici Lompounu KepLL

Data File : C:\MSDCHEM\1\5973N\02FEB04\00166.D Vial: 5 • Acq On : 4 Feb 2002 6:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 9.84 0.28 ug/L 173487 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 64 3 PROPYLENE GLYCOL TRIMER 3 174 C9H18O3 000000-00-0 64 4 3-Hexanol 102 C6H140 000623-37-0 40 Abundance Scan 566 (9.836 min): 00166.D (-) m/z 59.10 100.00% 59

5000

45 73 104 9.40 9.60 9.80 10.00 10.20 m/z-> 0- . W 40 30 . 1 —L 50__ 60 70 ■

80 i 84 '1 ■ ■ i 1 ■ 1 ■ i 1 1 ■ 1 » ■ ■ ■ • i ' ' • • i ■ 1

90 100 110 120 130 m/z 45.10 12.29% Abundance #43942:2-Propanol, 1-(2-methoxy propoxy)- $$ 1-(2-Methoxyp... 59 _...

5000 9.40 9.60 9.80 10.00 10.20 m/z 73.10 8.71% 31 45 0- -- 73..... 104 .... 130 •i 11 ■ * i 1 1 1 1 1 11■ >।i । । ■ । 1 1 1 1 1 1 11’11 1 niz-> 30 40 50 60 70 80 90 100 110 120 130

M. AM mAm Abundance #78532: PROPYLENE GLYCOL TRIMER 1 59 Ar 9.40 9.60 9.80 10.00 10.20 5000 41 m/ z 43.10 8.57% 103 A

73 R7 117 130 0- j — l m ------ 1 • ■ i ■ • ■ • I ■ 1 • * i ' ‘ miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78534: PROPYLENE GLYCOL TRIMER 3 59 9.40 9.60 9.80 10.00 10.20 m/ z 41.10 8.12%

5000 41 103

m/z-> 0 I, 73 87 117 130 > । । 1 1 ' 1 1 । 11 g I . l’ । । ( i i i'i । i-i i i J 1*41444141144 30 40 50 60 70 80 90 100 110 120 130 A 9.40 _A 9.60 9.80 10.00 10.20

)0166.D SCAN508.M Tue Feb 05 09:47:40 2002 Page 11

NYC-WTC_000050697

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