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GCMS analysis results for sample AE00110, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.

NYC-WTC_000050645–000050663

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document — **t ” ****

Data File : C:\MSDCHEM\1\5973N\02FEB04\00110.D Vial: 4 Acq On : 4 Feb 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C: \DATABASE\WILEY7N . L Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.34 ug/L 299651 Phenanthrene- dl 0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 95 2 Anthracene-D10 188 C14D10 000000-00-0 72 3 Cyclohept anone, 4-phenyl- 188 C13H16O 067688-28-2 47 4 Anthracene-dlO- 188 C14D10 001719-06-8 38 Abundance Scan 1699 (22.771 min): 00110.D (-) m/z 188.20 100.00% its

5000

80 94 [ 132 146 160 | mm 22.40 22.60 22.80 23.00 23.20 52 66 0- — ■ I ■ ! . . i 1 I 1 । 1’8 m/z 94.10 18.46% m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 m.. . 2240 22.60 22.80 23.00 23.20 80 94 m/z 80.10 13.54% 66 158 0- ■ * i»। ■ i • • l ■ i k -rt-TTrt pp m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D1 0 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 13.04% 80 94 66 160 — 6 ‘ ' M 11 ■' I > । ■ । ‘ 1 " I " 111'1" I “ " 1 rr ' “ 11' 111| “ 111 nz-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98298: Cycloheptanone, 4-phenyl- .. -................ , 117 its 22.40 22.60 22.80 23.00 23.20 104 m/z 184.10 12.94% 160 5000 131 170 145 0 TIT 11 “ 1 ■ i ‘ • i * ■ “ i " ‘ ‘ i' ’ 1’3 11 ‘ ‘T • ■ i • ■ I’T n/z—> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

)0110.D SCAN508.M Tue Feb 05 09:47:02 2002 Page 14

NYC-WTC_000050662

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NYC-WTC_000050662Source: NYC Law Department, mirrored locally

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