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GCMS blank analysis results for sample AE00110, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on February 4-7, 2002.

NYC-WTC_000050627–000050644

Folder label: “GCMS X 1/4/02 A 2/4/02

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Scanned page image, NYC-WTC_000050637
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB04\0204BB.D Vial: 1 Acq On : 4 Feb 2002 10:58 am Operator: Sample : lab blank l/4b Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 O-CHLOROPHENOL-D4 $$ 3,4,5,... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 9.24 0.10 ug/L 40888 1,4-Di chloroben z ene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual I 0-CHLOROPHENOL-D4 $$ 3,4,5,6-Tet... 132 C6HD4C1O 000000-00-0 80 2 (E)-3-Chloro-2-methyl-2-pentenal 132 C6H9C1O 031357-76-3 16 3 Xenon $$ Xe $$ UN 2036 $$ UN 259... 132 Xe 007440-63-3 9 4 4-Chloro-tetradeuteriophenol 132 C6HD4C10 000000-00-0 9 Abundance Scan 514 (9.242 min): 0204BB.D (-) m/z 132.00 100.00% 132

5000 68 93 40 63 86 / A 8.80 9.00 9.20 9.40 9.60 0- ■ ' i • ■ ■ ■ i ■ ■ i ' ' 1 1 i 1 ' • * i • > m/z 68.10 41.46% niz-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #24012:0-CHLOROPHENOL-D4 $$ 3,4,5,6-Tetradeuterio-2-chlor... 132

5000 68 8.80 9.00 9.20 9.40 9.60 96 m/z 134.00 34.95% 48 | 76 104 _______________1 1 0- ----PPP • i ■ ■ ■ ■ । ‘ ।1 ■ • i ‘ ■ miz-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #27731: (E)-3-Chloro-2-methyl-2-pentenal 132

8.80 9.00 9.20 9.40 9.60 67 m/z 93.00 34.03% 5000 97 53 117 79 0- 1 L 11 mfz-> 40 50 60 70 80 90 1(» 110 120 130 140 Abundance #28482: Xenon $$ Xe $$ UN 2036 $$ UN 2591 $$ Xenon, refrig... T 132 8.80 9.00 9.20 9.40 9.60 m/z 63.00 26.62% 5000

66 0 ----- ....... . ,/1241 ■ ■ i ' ■ m/z-> 40 50 60 70 80 90 100 110 120 130 140 8.80 9.00 9.20 9.40 9.60

204BB.D SCAN508.M Tue Feb 05 09:47:46 2002 Page 8

NYC-WTC_000050637

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NYC-WTC_000050637Source: NYC Law Department, mirrored locally

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