Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
NYC-WTC_000050596–000050614Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00250.D Vial: 6 • Acq On : 24 Jan 2002 7:06 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 1-Butanamine, 2-ethyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 23.81 0.07 ug/L 52992 Phenanthrene -dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l-Butanamine, 2-ethyl- 101 C6H15N 000000-00-0 9 00 2 1-METHYL-5-AMINO-D2-1,2,4-TRIAZOLE 100 C3H4D2N4 053778-60-2 9 3 1-Hexanamine $$ Hexylamine $$ n-... 101 C6H15N 000111-26-2 9 c 4 2,4-Imidazolidinedione (CAS) $$ ... 100 C3H4N202 000461-72-3 9 Abundance Scan 1790 (23.810 min): 00250. D (-) m/z 100.10 100.00% 100
5000
41, • (1155 86 188 23.40 23'.60 23.80 24.00 24.20 111 n 111 ■■ 11 ■’! r 11 m 11 r-r.) > d > 11 n ■■1 “ •■1"1 ‘ 1" “ 1 • ■1 ■ 1 “1 ■ i ■ ■ ■ ■ 1 ‘i■" l|' “ ■ m/z 41.10 6.01% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #9011:1 -Butanamine, 2-ethyl- 33
5000 23*40 23.60 23.80 24.00' 24.20 m/z 43.10 5.55% ,43 55 72 84 192 N ‘1’58 ■' ’ ' l11 ■ ■ | ‘'111 “ ‘' 11'1' I'1'' I “ “ l’1'' ‘11' n 111 " I " " I " 1 T'' p 1 n-f 11 rrp 1 it) > 1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #6725:1-METHYL-5-AMlNO-D2-1,2,4-TRlAZOLE 100 I ■ ‘ 1 1 1 ' • • l • 4 I ■ ■ ■ ‘ I ' ‘ 23.40 23.60 23.80 24.00 24.20 5000 m/z55.10 5.01% 45 56
Tmp 30 1 ,.. 72..... | D’1—0010000uu"BTTtrtont * t ■' ‘ ■ i * ■1 ‘ i''1 • i > *'1 nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #8933:1-Hexanamine $$ Hexylamine $$ n-Hexylamine $$ Mono-... ■ ' i ■ ‘ ■ i • ■ 33 23.40 23.60 23.80 24.00 24.20 m/z 86.10 4.40% 5000
t 44 55..... 72 ......... 101............................................ 'I'"1 ■I . > 1!"44 । | . .1 । | I I M | I .. I | | | | | I I I I | I I I I | I ! I ! | I | I I | I I 1 1 |! U t | | I T ( ‘ l 1 ' ‘ ‘ I ‘ ‘ miz—> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 23.40 23.60 23.80 24.00 24.20
3250.D SCAN508.M Fri Jan 25 10:26:24 2002 Page 13
NYC-WTC_000050612
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006126
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder