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GCMS analysis results for sample AE00169, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050519–000050538

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050525
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NYC 9/11 Public Portal Document **rX**

Data .File : C:\MSDCHEM\l\5973N\02JAN24\00169.D Vial: 2 . Acq On : 24 Jan 2002 3:48 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 3.50 0.15 ug/L 75350 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 56 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 50 Abundance Scan 11 (3.499 min): 00169.D (-) m/z 74.00 100.00% 74

82 5000 47 39 86 3.50 3.60 3.70 3.80 3.90 ''1 mHHH TTPTTTTTTH 11 ] 1... j(।।. m/z 81.90 56.76% m/z—> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 -A i’*’’1’’14111441****I 3.50 3.60 3.70 3.80 3.90 47 m/z 84.00 37.58% -MTT ‘ ‘I‘ 1 1,1 ■ “ i ■ ■ “ i “ “ r ■ • • i “109 "i“ ■ ■ i •■ ■ m/z—> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #11644: Acetonitrile, dichloro- 74 35 3.50 3.60 3.70 3.80 3.90 ''' 5000 82 m/z 76.00 34.54% 47 40 •-mi | >> ■1 t "‘■I mmpt T "'I' m/z—> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 0 3.50 3.60 3.70 3.80 3.90 m/ z 47.00 23.07% 47 82 5000

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)0169.D SCAN508.M Fri Jan 25 10:25:58 2002 Page 3

NYC-WTC_000050525

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NYC-WTC_000050525Source: NYC Law Department, mirrored locally

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