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GCMS analysis results for sample AE00168, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050500–000050518

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050517
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\O2JAN24\00168.D Vial: 1 Acq On : 24 Jan 2002 2:59 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.32 ug/L 234038 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW Mol Form . CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Anthracene-dlO- 188 C14D10 001719-06-8 64 4 Acridine-D9 188 C13D9N 000000-00-0 59 Abundance Scan 1699 (22.771 min): 00168. D (-) m/z 188.10 100.00% 188

5000

94 ------ 80 54 66 132 160 | 22.40 22,60 22.80 23.00 23.20 r । ■ 11111111111.1111 ■. 11 |'I 1*PTD*LPIIH 1’8 m/z94.10 19.17% mz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

................................................ 5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.10 15.45% 66 i ‘11 ■ i1 ■ ■ ■ i ■11 ■ i • ■ 1 • J •“> 111 । । 158 j .ti i । i i i i । 1 i I I | i i i i । .... । . i 1' TTT miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 1(8 . .............................................. 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.15 13.86%

80 94 160

n/z-> 40 66 ।■ i' ■ ■ ■ i “' ■ i “

50 60 70 —80 90 h III.... 19111 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- --------- 1(8 22.40 22.60 22.80 23.00 23.20 m/z 184.10 13.28%

5000

66 80 94 160 niz-> 40 50 I" 111" -----1804— -------- 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

)0168.D SCAN508.M Fri Jan 25 10:25:54 2002 Page 14

NYC-WTC_000050517

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NYC-WTC_000050517Source: NYC Law Department, mirrored locally

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