Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
NYC-WTC_000050481–000050499Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document a1X Dcat’ii wpOuIL KCPOL L
Data File: C:\MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 • Acq On : 24 Jan 2002 2:09 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.06 ug/L 1975320 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 Abundance Scan 220 (5.885 min): 00167.0 (-) m/ z 73.10 100.00% 73
5000 43
। | 55 . 87 b rp"i i rp . i ! 11 i rrplhn" i j n’’tpi . i i'i'i'I-. < । . MIT 103 11 1 ■ i •'1 ■ i ■ ‘‘ i' “1 > ■ ‘ । > j... । p.. > (i m/z ' ■ i • ■ 5.60 , " d 1 span 43.10 5.80 I 6.00 6.20 24.64% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73
I 5000 ■ ■ i 1 ■ ‘ ' i ' ■ ' * i ■~ 1 1 I ' ‘ 5.60 5.80 6.00 6.20 43 m/z 45.10 9.20% 27 87 113 174 spunnipunaga ,. ’.I’l’e. p55 ri । p ree. ++ss4tt+1+t**1****)*ddG1G**1***Y* u p 1 ■ l"| I I I I | I I I I | I miz-> 10 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 * I ■ • • i ‘ • * ■ i7 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.07% 43 .................................. 27 87 TTt ■ i'55 । ■ ■ ■ i ■ ■ •11 ■ Tprtj 174 113 • i • • • >i* < <•i> <•»।>•••i “«• i•■ • •i “ • • i “ “ i • mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... nnn 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.56%
5000 44 58 15 n/z—> T mhp l1' “ i1 1111 < 1111»11 > 11 • < > 11 ri 11 r 111111 n-f 11111 1i1 p rinpuip 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 A *]■•••!•••• | •! । i | < i 5.60 5.80 6.00 6.20
>0167.D SCAN508.M Fri Jan 25 10:25:47 2002 Page 9
NYC-WTC_000050493
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NYC-WTC_000050596
Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder