GCMS blank analysis results for sample AE00167, Jan 2002

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Data File : C:\MSDCHEM\1\5973N\02JAN24\0104B.D Vial: 1 Acq On : 24 Jan 2002 11:41 am Operator: Sample : lab blankl/4 Inst : Instrumen Mise : January 24’, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Buten-l-ol, 2-methyl- (CA... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.63 0.04 ug/L 14352 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-l-ol, 2-methyl- (CAS) $$... 86 C5H10O 004675-87-0 45 2 1-Butene, 1-methoxy- $$ Ether, 1... 86 C5H10O 029512-02-5 9 3 1-Butene, 1-methoxy- (CAS) $$ ME... 86 C5H10O 029512-02-5 9 4 2-Butene, 1-methoxy-, (E)- $$ Et... 86 C5H10O 010034-14-7 9 Abundance Scan 110 (4.630 min): 0104B.D (-) m/z 71.10 100.00% 71 88 41 57 5000 T-r-pr-r-r-r-pt-r-T i ' 1 1 1 i ■ 11 T 1 4.20 4.40 4.60 4.80 5.00 51 m/z 88.10 62.58% ‘1′7711111111 " i ■ ■ ■ ■ i ‘ “ i -rr-p-rr-r-p-r ■ i ■ ■ ■ ■ i ■' ■ ■ i • ■ ‘ ■ i ■ • ■ ■ i • ■ ■ i " • ■ i ■ ■ ■ ■ i ■ miz-> 2025303540 45 5055 60 65 70 75 80 85 90 95 Abundance #4064:2-Buten-1-ol, 2-methyl- (CAS) $$ 2-Methyl-but-2-ene... 71

5000 43 86 ■ • i ■ ■ • ■ i ■ ■ 1 4.20 4.40 4.60 4.80 5.00 39 53 m/z 41.10 53.03% 57 67 ■ ■ 11' ' I' 11 ■ I' ■ ■' l' 11.1 '1111" i'11111" 111' -rp-r I ■. I. ■ ■ ■ I ■».. I ■n-p-n-r-p-r mz-> 20 25 30 35 40 45 50556065 70 75 80859095 Abundance #4105:1-Butene, 1-methoxy- $$ Ether, 1-butenyl methyl $$ ... 7h 4.20 4.40 4.60 4.80 5.00 41 86 m/ z 57.10 50.25% 5000

27 45 55

mz-> 20 " I" 111.31.007 Im Mii me 1111 ■ 11 p 111 p 1111 1-rr-pn-rrprr 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4104:1-Butene, 1-methoxy- (CAS) $$ METHYL BUT-1-ENYL ETH... i ■ ■ 1 ' i ' ■ ■ ' i 71 4.20 4.40 4.60 4.80 5.00 m/z 86.00 41.47%

5000

27 41

55 86 MMWw/w/ 1 31 45 I l । i t < i j t “ i1 • ■ ■ i ■ ■ ■ ■ i 1111111'111 ‘" 11,11111" I -rp-m-p-r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.20 4.40 4.60 4.80 5.00

)104B.D SCAN508.M Fri Jan 25 10:26:29 2002 Page 6

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