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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/24 - 1/25/02
Document / 37 pages

GCMS blank analysis results for sample AE00167, Jan 2002

Machine-extracted title · confidence 100%

Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.

NYC-WTC_000050444–000050480

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050479
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LLJLGy DCaLtii ~pourau a\SpL

Data File : C:\MSDCHEM\l\5973N\02JAN25\0104B2.D Vial: 4 Acq On : 25 Jan 2002 12:39 pm Operator: Sample : lab blank 1/4; 2nd inj. Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 dichloromethane $$ Methane,... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 39.05 0.05 ug/L 18624 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 dichloromethane $$ Methane, dich... 84 CH2C12 058165-12-1 7 2 Methane, dichloro- (CAS) $$ Dich... 84 CH2C12 000075-09-2 7 3 Methane, dichloro- (CAS) $$ Dich... 84 CH2C12 000075-09-2 7 4 Methane, dichloro- (CAS) $$ Dich... 84 CH2C12 000075-09-2 7 Abundance Scan 3125 (39.051 min): 0104B2.D (-) m/z 96.00 100.00% 49 96

5000 84 191 281 MM / N MA , 208 38.80 39.00 39.20 39.40 i ■ ■111 '11 '1 ‘ i i ■ ■ ■ ■ i • • ‘ ■ i ■ ■'' i ■ ■ ■ • i ■ ■ ■ ■ i ■ •' i ■ ■ • ■ i ■' • ■ i • ■ ■' I m/z 49.00 96.52% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 49 #3073: dichloromethane $$ Methane, dichloro-, radical ion(... MA N

84 5000] ■ ■ I 1T 38.80 39.00 39.20 39.40 m/z 191.00 78.45% ■ ■ ■ l . n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #3064: Methane, dichloro- (CAS) $$ Dichloromethane $$ R 30... 49 84 38.80 39.00 39.20 39.40 5000 m/z 281.00 74.19%

35 । 1. . J A | | | | 1 |“| T l 1 | 1 I I l | a a —0020 0/ miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #3067: Methane, dichloro- (CAS) $$ Dichloromethane $$ R 30... 49 m/z 83.90 65.81% 84 J 5000

27.1/14 '11 ■' ‘ ■ i 11 ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ • ■ i ■ ■ ■111'11111'' i111 ■ i'1 ■ ■ I' ■111 ■ ■ ’"I ■ ' i7 ' * * i * • m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 38.80 39.00 39.20 39.40

3104B2.D SCAN508.M Fri Jan 25 13:22:51 2002 Page 15

NYC-WTC_000050479

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NYC-WTC_000050479Source: NYC Law Department, mirrored locally

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