GCMS blank analysis results for sample AE00167, Jan 2002

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Data File : C:\MSDCHEM\1\5973N\02JAN25\0104B2.D Vial: 4 Acq On : 25 Jan 2002 12:39 pm Operator: Sample : lab blank 1/4; 2nd inj. Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.18 ug/L 104784 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 3 Acridine-D9 188 C13D9N 000000-00-0 72 4 Phenanthrene-diO 188 C14D10 001517-22-2 64 Abundance Scan 1699 (22.771 min): 0104B2.D (-) m/z 188.10 100.00% 188

5000

44 54 66 80 , *4 146 10 u 22.40 22.60 22.80 23.00 23.20 | | | 1 1 I ; | t f | > | ! I I i P t I t [ « I | I [ I h { | t l l t | | : 4 1 | > | 1 1 | 1 11 I } I l t | | l t H‘| 1 I PT J T T! 1 | I I’r’l Illi m/z 94.10 13.08% niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

5000 2240 22.60 22.80 23.00 23.20 m/z 184.10 11.09% 66 TIWmTTTTTTTTTTTTT ■ ‘ i' “ ■ i ■ 3 160 11111101111189, . i. miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 . A. . 22.40 22.60 22.80 23.00 23.20 50)0 m/z 160.10 10.23%

80 94 ■ ■ i ‘ 66 - ■ i “ ■ i ■ ‘1 ■ i “

m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 158 22.40 22.60 2280 23.00 23.20 m/z 189.15 10.01%

5000

mfz-> 66,80.1 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 4 PH . /.A,__ 22,40 22.60 22.80 23.00 23.20

0104B2.D SCAN508.M Fri Jan 25 13:22:50 2002 Page 14

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