GCMS blank analysis results for sample AE00167, Jan 2002

NYC 9/11 Public Portal Document L31a1 y Dcati Mupouru NSpUL

Data File : C:\MSDCHEM\1\5973N\02JAN25\0104B2.D Vial: 4 Acq On : 25 Jan 2002 12:39 pm Operator: Sample : lab blank 1/4; 2nd inj. Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 1,3,5,7-Tetraazatricyclo[3 .... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.

16.55 0.03 ug/L 18194 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,5,7-Tetraazatricyclo [3.3.1.1.. . 140 C6H12N4 000100-97-0 7 2 Methylphloroglucinol 140 C7H803 000000-00-0 5 3 Methenamine $$ 1,3,5,7-Tetraazaa... 140 C6H12N4 000100-97-0 5 4 2-Dimethylamino-4,5-dimethyl-oxa... 140 C7H12N20 000000-00-0 4 Abundance Scan 1154 (16.549 min): 0104B2.D (-) m/z 140.20 100.00% 140

5000

122 172 Ii 43 71 16.20 16.40 16.60 16.80 1 I •' i ■ • ■' i ■1 • • i' ■ ■ ■ i • “ ‘ i ■' • ■ i ■ •" i ■ ‘ 84 ■ i • ‘ ■ i ■ ■ ■ ‘ i ■ “ • i ■ ■ ■' i • • i" ' • i" “ i1 ■ ‘ 1- m/z 172.20 22.73% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35203:1,3,5,7-Tetraazatricyclo[3.3.1.1 (3,7)Jdecane (CAS)... 140

85 5000 16.20 16.40 16.60 16.80 112 m/z 122.10 22.11% 71 .................. 58 I ■■i" ' ‘ i ■ “ ‘ i ■ ■" i ■ “ ' i' • ■11 ■ ■ ■ 'i' ...... mmppmp n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35391: Methylphloroglucinol 1 0

16.20 16.40 16.60 16.80 5000 m/z 138.20 19.80% 111 123 66 85 94 ........... ............. T...... I,,, J .1,... 1 ». t .... I।। p 11 H ...»111 I 111 ।. .i. । » 144 ( 111 । 111 । 111 ■ ■ i “ ■ ■ i ■ ■ ■ ■ i ■" ■ i1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35198: Methenamine $$ 1,3,5,7-Tetraazaadamantane $$ 1,3,5... T T }ir 42 16.20 16.40 16.60 16.80 m/z 71.00 15.22%

5000 140

15 I 30 71 ‘ ‘ I ‘ ‘‘' I ‘' 1*' • 13 . ।।। fl 11111111 > 11 85 ■11" " i11 ■' i ■" ■ i1 112 ■ ■ i 1 ■ 1 ■ i ■ ■ 1***1*‘‘I* miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16,20 16,40 16.60 16.80

)104B2.D SCAN508.M Fri Jan 25 13:22:50 2002 Page 12

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