GCMS calibration analysis for sample AE00167, Jan 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN24\0124C40.D Vial: 2 Acq On : 24 Jan 2002 9:58 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 24 10:54:22 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1415024 20.00 ug/L 0.00 10) Naphthalene-d8 13.21 136 6045986 20.00 ug/L 0.00 17) Acenaphthene-diO 18.35 164 3104960 20.00 ug/L 0.00 29) Phenanthrene-diO 22.66 188 5466763 20.00 ug/L -0.01 38) Chrysene-dl2 30.52 240 4895611 20.00 ug/L 0.01 44) Perylene-dl2 34.43 264 3599824 20.00 ug/L 0.01 System Monitoring Compounds 37) 2,4-DDD 27.58 235 43173 0.50 ug/L -0.15 Spiked Amount 5.000 Recovery = 10.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 2618532 43.42 ug/L 54 3) bis(2-Chloroethyl)ether 9.28 93 3240229 36.03 ug/L 84 4) 1,3-Dichlorobenzene 9.62 146 3888463 36.63 ug/L 96 5) 1,4-Dichlorobenzene 9.77 146 3813543 35.77 ug/L 98 6) 1,2-Dichlorobenzene 10.25 146 3142735 33.20 ug/L 100 7) 2,2'-oxybis (1-Chloropropa 10.69 45 5341823 32.64 ug/L 96 8) n-Nitroso-di-n-propylamine 11.09 70 2340731 (31.34 ug/L 83 9) Hexachloroethane 11.03 117 1313365 34.41 ug/L 98 11) Nitrobenzene 11.38 77 3759002 33.30 ug/L 88 12) 1sophorone 12.05 82 7213237 35.42 ug/L 94 13) bis(2-Chloroethoxy)methane 12.79 93 4662174 38.52 ug/L 93 14) 1,2,4-Trichlorobenzene 13.13 180 2799582 35.51 ug/L 97 15) Naphthalene 13.27 128 10256735 35.42 ug/L 99 16) Hexachlorobutadiene 13.85 225 1338828 (31.94 g/L 98 18) Hexachlorocyclopentadiene 15.97 237 748037 (2696 ug/L 97 19) 2-Chloronaphthalene 16.67 162 5922936 34.54 ug/L 94 20) Dimethylphthalate 17.92 163 6750477 32.92 ug/L 96 21) 2,6-Dinitrotoluene 18.09 165 1485283 37.14 ug/L 84 22) Acenaphthylene 17.88 152 9133138 36.53 ug/L 99 2 3) Acenaphthene 18.44 153 5535140 3107 ug/L 98 24) 2,4-Dinitrotoluene 19.22 165 2086855 39.85 ug/L 92 25) Diethylphthalate 20.03 149 6166367 <31.38 ug/L 98 26) 4-Chlorophenyl-phenylether 20.04 204 2620331 <3173 ug/L 94 27) Fluorene 19.94 166 7117195 35.13 ug/L 99 28) Azobenzene/1,2-Diphenylhyd 20.50 77 8630007 35.23 ug/L 87 30) N-nitrosodiphenylamine 20.46 169 4453080 32.11 ug/L 97 31) 4-Bromophenyl-phenylether 21.46 248 1910436 33.58 ug/L 92 32) Hexachlorobenzene 21.80 284 1969476 32.76 ug/L 96 3 3) Phenanthrene 22.73 178 10392743 34.50 ug/L 100 34) Anthracene 22.86 178 10370458 35.49 ug/L 100 (#) = qualifier out of range (m) = manual integration 0124C40.D SCAN508.M Thu Jan 24 10:54:22 2002 Page 1

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