GCMS results for sample AE00703, Jan 17 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN16\0116C40.D Vial: 2 Acq On : 16 Jan 2002 9:12 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 16 10:15:23 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1171718 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 5011586 20.00 ug/L -0.01 17) Acenaphthene-diO 18.35 164 2680558 20.00 ug/L 0.00 29) Phenanthrene-diO 22.66 188 4944155 20.00 ug/L -0.01 38) Chrysene-dl2 30.52 240 4220678 20.00 ug/L 0.01 44) Perylene-dl2 34.43 264 3150025 20.00 ug/L 0.01

System Monitoring Compounds 37) 2,4-DDD 27.58 235 38191 0.49 ug/L -0.15 Spiked Amount 5.000 Recovery = 9.80%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.98 74 2140519 42.87 ug/L 54 3) bis(2-Chloroethyl)ether 9.26 93 2707225 36.36 ug/L 77 4) 1,3-Dichlorobenzene 9.62 146 3184941 36.23 ug/L 96 5) 1,4-Dichlorobenzene 9.77 146 3154882 35.73 ug/L 98 6) 1,2-Dichlorobenzene 10.25 146 2639468 33.67 ug/L 100 7) 2,2'-oxybis (1-Chloropropa 10.68 45 4491427 33.14 ug/L 95 8) n-Nitroso-di-n-propylamine 11.08 70 1938539 <3135 ug/L 83 9) Hexachloroethane 11.03 117 1106709 35.01 ug/L 97 11) Nitrobenzene 11.38 77 3053882 32.63 ug/L 86 12) Isophorone 12.04 82 5941224 35.19 ug/L 95 13) bis(2-Chloroethoxy)methane 12.79 93 3860309 38.47 ug/L 93 14) 1,2,4-Trichlorobenzene 13.12 180 2322914 35.55 ug/L 98 15) Naphthalene 13.26 128 8590607 35.79 ug/L 99 16) Hexachlorobutadiene 13.85 225 1117734 32.17 ug/L 99 18) Hexachlorocyclopentadiene 15.95 237 806474 33.67 ug/L 99 19) 2-Chloronaphthalene 16.67 162 5000162 33.78 ug/L 94 20) Dimethylphthalate 17.92 163 5775788 32.63 ug/L 95 21) 2,6-Dinitrotoluene 18.09 165 1317214 38.15 ug/L 80 22) Acenaphthylene 17.88 152 7848423 36.36 ug/L 99 23) Acenaphthene 18.44 153 4753988 30.92Jug/L 100 24) 2,4-Dinitrotoluene 19.22 165 1941674 42.94 ug/L 88 25) Diethylphthalate 20.03 149 5421435 31.96 ug/L 99 26) 4-Chlorophenyl-phenylether 20.04 204 2307677 32.37 ug/L 92 27) Fluorene 19.94 166 6237935 35.67 ug/L 98 28) Azobenzene/1,2-Diphenylhyd 20.50 77 7447240 35.21 ug/L 86 30) N-nitrosodiphenylamine 20.46 169 3986300 31.78 ug/L 99 31) 4-Bromophenyl-phenylether 21.46 248 1697949 33.00 ug/L 90 32) Hexachlorobenzene 21.80 284 1789490 32.91 ug/L 97 33) Phenanthrene 22.73 178 9273460 34.04 ug/L 99 34) Anthracene 22.86 178 9260446 35.04 ug/L 100

(#) = qualifier out of range (m) = manual integration 0116C40.D SCAN508.M Wed Jan 16 10:15:23 2002 Page 1

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