GCMS calibration results for sample AE00555, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

, Data File : C:\MSDCHEM\1\5973N\02JAN29\0129C40.D Vial: 2 Acq On : 29 Jan 2002 9:15 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 29 10:10:59 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1554403 20.00 ug/L 0.00 10) Naphthalene-d8 13.22 136 6716204 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.35 164 3442983 20.00 ug/L 0.00 29) Phenanthrene-diO 22.66 188 5724598 20.00 ug/L -0.01 38) Chrysene-dl2 30.51 240 4823919 20.00 ug/L 0.00 44) Perylene-dl2 34.43 264 3675361 20.00 ug/L 0.01

System Monitoring Compounds 37) 2,4-DDD 27.58 235 43065 0.48 ug/L -0.15 Spiked Amount 5.000 Recovery = 9.60%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 2900418 43.78 ug/L 54 3) bis(2-Chloroethyl)ether 9.28 93 3603436 36.48 ug/L 84 4) 1,3-Dichlorobenzene 9.62 146 4287722 36.76 ug/L 97 5) 1,4-Dichlorobenzene 9.77 146 4177297 35.66 ug/L 99 6) 1,2-Dichlorobenzene 10.25 146 3489193 33.55 ug/L 99 7) 2,2'-oxybis (l-Chloropropa 10.69 45 5926748 32.97 ug/L 96 8) n-Nitroso-di-n-propylamine 11.09 70 2592630 <31.60/ ug/L 84 9) Hexachloroethane 11.03 117 1491670 35.57 ug/L 99 11) Nitrobenzene 11.38 77 4205810 33.54 ug/L 88 12) Isophorone 12.05 82 8074580 35.69 ug/L 94 13) bis(2-Chloroethoxy)methane 12.79 93 5203156 38.69 ug/L 94 14) 1,2,4-Trichlorobenzene 13.14 180 3079734 35.17 ug/L 98 15) Naphthalene 13.27 128 11276983 35.05 ug/L 99 16) Hexachlorobutadiene 13.85 225 1489292 31.98 ug/L 98 18) Hexachlorocyclopentadiene 15.96 237 986971 32.08 ug/L 100 19) 2-Chloronaphthalene 16.67 162 6447795 33.91 ug/L 96 20) Dimethylphthalate 17.92 163 7392551 32.51 ug/L 97 21) 2,6-Dinitrotoluene 18.09 165 1697815 38.28 ug/L 86 22) Acenaphthylene 17.88 152 10026533 36.16 ug/L 99 23) Acenaphthene 18.44 153 6057206 <30.67ug/L 99 24) 2,4-Dinitrotoluene 19.22 165 2344124 40.36 ug/L 91 25) Diethylphthalate 20.03 149 6702378 30.76 ug/L 99 26) 4-Chlorophenyl-phenylether 20.04 204 2813717 3073ug/L 94 27) Fluorene 19.94 166 7704464 34.30 ug/L 97 28) Azobenzene/1,2-Diphenylhyd 20.50 77 9335177 34.36 ug/L 88 30) N-nitrosodiphenylamine 20.46 169 4760488 32.78 ug/L 99 31) 4-Bromophenyl-phenylether 21.46 248 2029866 34.07 ug/L 91 32) Hexachlorobenzene 21.80 284 2099999 33.36 ug/L 96 33) Phenanthrene 22.73 178 10822588 34.31 ug/L 99 34) Anthracene 22.86 178 10778216 35.22 ug/L 100

(#) = qualifier out of range (m) = manual integration 0129C40.D SCAN508.M Tue Jan 29 10:10:59 2002 Page 1

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