GCMS calibration results for sample AD31647, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\l\5973N\02JAN22\0122C40.D Vial: 2 Acq On : 22 Jan 2002 9:26 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 22 15:29:54 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 9.73 152 1525665 20.00 ug/L 0.01 10) Naphthalene-d8 13.22 136 6804482 20.00 ug/L 0.00 17) Acenaphthene-diO 18.35 164 3657887 20.00 ug/L 0.00 29) Phenanthrene-diO 22.66 188 6333483 20.00 ug/L -0.01 38) Chrysene-dl2 30.52 240 5183286 20.00 ug/L 0.01 44) Perylene-dl2 34.44 264 4026343 20.00 ug/L 0.02

System Monitoring Compounds 37) 2,4-DDD 27.58 235 44852 0.45 ug/L -0.15 Spiked Amount 5.000 Recovery = 9.00%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.98 74 2825090 43.45 ug/L 56 3) bis(2-Chloroethyl)ether 9.28 93 3378686 34.83 ug/L 81 4) 1,3-Dichlorobenzene 9.62 146 4156694 36.31 ug/L 97 5) 1,4-Dichlorobenzene 9.77 146 4011180 34.89 ug/L 99 6) 1,2-Dichlorobenzene 10.25 146 3297216 32.30 ug/L 99 7) 2,2'-oxybis (1-Chloropropa 10.69 45 5766011 32.68 ug/L 95 8) n-Nitroso-di-n-propylamine 11.10 70 2652674 32.95 ug/L 85 9) Hexachioroethane 11.03 117 1455973 35.37 ug/L 98 11) Nitrobenzene 11.39 77 4197185 33.03 ug/L 86 12) Isophorone 12.06 82 8438620 36.82 ug/L 94 13) bis(2-Chloroethoxy)methane 12.80 93 5271514 38.69 ug/L 93 14) 1,2,4-Trichlorobenzene 13.14 180 3046020 34.33 ug/L 97 15) Naphthalene 13.27 128 11383496 3493 ug/L 99 16) Hexachlorobutadiene 13.85 225 1487717 ?!. 54 ug/L 99 18) Hexachlorocyclopentadiene 15.97 237 1210864 3 ug/L 97 19) 2-Chioronaphthalene 16.67 162 6782351 33.58 ug/L 97 20) Dimethylphthalate 17.93 163 7965019 32.97 ug/L 97 21) 2,6-Dinitrotoluene 18.10 165 1940427 41.18 ug/L 83 22) Acenaphthylene 17.88 152 10547376 35.81 ug/L 98 2 3) Acenaphthene 18.46 153 6344379 30.23 ug/L 100 24) 2,4-Dinitrotoluene 19.23 165 2757705 44.7 ug/L 94 25) Diethylphthalate 20.04 149 6863810 29.6 ug/L 98 26) 4-Chlorophenyl-phenylether 20.05 204 2933841 30.1 ug/L 93 27) Fluorene 19.94 166 8232776 34.5 ug/L 97 2 8) Azobenzene/1,2-Diphenylhyd 20.51 77 9490137 32.88 ug/L 87 30) N-nitrosodiphenylamine 20.49 169 4880611 30.38 ug/L 99 31) 4-Bromophenyl-phenylether 21.46 248 2186567 33.18 ug/L 94 32) Hexachlorobenzene 21.80 284 2277042 32.69 ug/L 99 3 3) Phenanthrene 22.74 178 11569475 33.15 ug/L 99 34) Anthracene 22.87 178 11531459 34.06 ug/L 100 (#) = qualifier out of range (m) = manual integration 0122C40.D SCAN508.M Tue Jan 22 15:29:54 2002 Page 1

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