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GCMS calibration analysis for sample AE00167, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.

NYC-WTC_000050435–000050438

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN24\0124C40.D Vial: 2 Acq On : 24 Jan 2002 9:58 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 24 10:54:22 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Compound R.T. Qlon Response Cone Unit Qvalue 35) Di-n-butylphthalate 24.87 149 13015635 36.93 ug/L 99 3 6) Fluoranthene 26.25 202 11672567 39.26 ug/L 97 3 9) Pyrene 26.88 202 12131564 31.16 ug/L 98 40) Butylbenzylphthalate 29.27 149 6012129 33.73 ug/L 99 41) Benzo(a)anthracene 30.47 228 10707264 36.25 ug/L 100 42) Bis(2-ethylhexyl)phthalate 31.12 149 7983214 35.37 ug/L 97 43) Chrysene 30.60 228 8372077 29.29 ug/L 98 45) Di-n-octylphthalate 32.85 149 13620125 40.33 ug/L 100 4 6) Benzo(b)fluoranthene 33.48 252 10379139 36.38 ug/L 98 47) Benzo(k)fluoranthene 33.56 252 9721627 35.65 ug/L 98 4 8) Benzo(a)pyrene 34.29 252 9527080 40.77 ug/L 97 49) Indeno (1,2,3-cd) pyrene 37.06 276 9664534 49.24 ug/L 91 5 0) Dibenz(a,h)anthracene 37.16 278 7606182 43.30 ug/L 97 51) Benzo(g,h,i)perylene 37.78 276 7992549 44.04 ug/L 94

(#) = qualifier out of range (m) = manual integration 0124C40.D SCAN508.M Thu Jan 24 10:54:22 2002 Page 2

NYC-WTC_000050437

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NYC-WTC_000050437Source: NYC Law Department, mirrored locally

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