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GCMS analysis results for sample AE00010, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00010 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050135–000050144

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050140
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN2402\10.D Vial: 13 Acq On : 25 Jan 2002 12:50 am Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.434 256 260 292 rVB 319358 993102 13.19% 2.622% 2 11.482 696 701 720 rBV 2328064 5785093 76.81% 15.272% 3 14.126 984 989 995 rBV 90215 177488 2.36% 0.469% 4 15.081 1087 1093 1111 rBV 3530549 7300215 96.92% 19.271% 5 20.341 1660 1666 1692 rBV 3631512 7531902 100.00% 19.883%

6 24.757 2141 2147 2159 rBV2 3303066 6926477 91.96% 18.285% 7' 29.834 2695 2700 2708 rBV 389092 756773 10.05% 1.998% 8 32.781 3015 3021 3043 rBV2 2011669 4812769 63.90% 12.705% 9 36.847 3456 3464 3483 rBV 1328751 3597203 47.76% 9.496%

Sum of corrected areas: 37881022

10.D GCMS0208.M Fri Feb 08 13:36:07 2002

NYC-WTC_000050140

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NYC-WTC_000050140Source: NYC Law Department, mirrored locally

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