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GCMS analysis results for sample AE00104, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00104 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050155–000050164

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050160
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN2402\104.D Vial: 15 Acq On : 25 Jan 2002 2:47 am Operator: 209 GALOS Sample. : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.428 256 260 295 rVB 269072 851318 13.90% 2.706% 2 11.486 697 702 727 rBV 1791346 4723671 77.10% 15.016% 3 14.130 985 990 996 rBV 183548 343180 5.60% 1.091% 4 15.075 1088 1093 1109 rBV 2891416 5976909 97.55% 19.000% 5 20.345 1661 1667 1687 rBV 2904714 6126778 100.00% 19.476%

6 24.751 2141 2147 2160 rBV2 2658899 5730319 93.53% 18.216% 7 29.837 2695 2701 2707 rBV 312551 646731 10.56% 2.056% 8 32.784 3015 3022 3046 rBV2 1679043 3964819 64.71% 12.604% 9 36.842 3455 3464 3486 rBV2 1120164 3094128 50.50% 9.836%

Sum of corrected areas: 31457853

104.D GCMS0208.M Fri Feb 08 13:37:50 2002

NYC-WTC_000050160

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NYC-WTC_000050160Source: NYC Law Department, mirrored locally

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