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GCMS analysis results for sample AD31457, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31457 conducted on February 13, 2002.

NYC-WTC_000018353–000018361

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018358
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31457.D Vial: 14 Acq On : 17 Jan 2002 12:20 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last. PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.447 258 262 295 rVB 438532 1243167 18.14% 3.443% 2 11.495 698 703 723 rBV 2056073 5323208 77.67% 14.741% 3 15.094 1089 1095 1113 rBV 3212802 6671433 97.34% 18.475% 4 20.354 1661 1668 1687 rBV 3271688 6853446 100.00% 18.979% 5 24.770 2143 2149 2162 rBV2 2975621 6470100 94.41% 17.917%

6 26.799 2364 2370 2378 rBV 43292 90301 1.32% 0.250% 7 29.847 2697 2702 2710 rBV 495394 969776 14.15% 2.686% 8 32.803 3017 3024 3046 rBV2 2035541 4789443 69.88% 13.263% 9 36.860 3459 3466 3486 rBV 1301468 3700164 53.99% 10.247%

Sum of corrected areas: 36111038

31457.D GCMS0103.M Thu Feb 07 09:17:50 2002

NYC-WTC_0000 18358

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NYC-WTC_000018358Source: NYC Law Department, mirrored locally

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