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GCMS unknown compounds report, sample AD31459, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP sample AD31459 identifying unknown compounds and surrogate recovery results from February 13, 2002.

NYC-WTC_000016533–000016542

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31459.D Vial: 15 Acq On : 17 Jan 2002 1:19 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.444 257 261 294 rBV 383990 1132137 16.30% 3.146% 2 11.272 674 678 692 rVB 30845 87931 1.27% 0.244% 3 11.502 698 703 723 rBV 2137910 5420830 78.06% 15.063% 4 15.091 1089 1094 1113 rBV 3265793 6711293 96.64% 18.649% 5 20.361 1661 1668 1688 rBV 3305411 6944360 100.00% 19.297%

6 24.776 2142 2149 2160 rBV2 2862600 6429424 92.58% 17.866% 7 29.853 2696 2702 2710 rBV 400635 824356 11.87% 2.291% 8 32.800 3017 3023 3040 rBV2 2058203 4708432 67.80% 13.083% 9 36.867 3458 3466 3485 rBV2 1347099 3728794 53.70% 10.361%

Sum of corrected areas: 35987557

31459.D GCMS0103.M Thu Feb 07 09:30:03 2002

NYC-WTC_000016538

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NYC-WTC_000016538Source: NYC Law Department, mirrored locally

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