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GCMS sample analysis report, Feb 2002

Machine-extracted title · confidence 80%

Gas chromatography mass spectrometry report documenting analytical results for environmental samples processed in mid-February 2002.

NYC-WTC_000016625–000016634

Folder label: “GCMS X 12/31/01 A 1/18/02

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Scanned page image, NYC-WTC_000016630
OCR text

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31504.D Vial: 12 Acq On : 19 Jan 2002 2:21 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.447 258 262 274 rBV 279442 747726 12.21% 2.359% 2 7.585 274 277 294 rVB 37798 165232 2.70% 0.521% 3 11.496 698 703 724 rBV 1813831 4848236 79.20% 15.293% 4 15.094 1089 1095 1114 rBV 2889647 5997495 97.97% 18.918% 5 20.355 1662 1668 1687 rBV 2951357 6121722 100.00% 19.310%

6 24.771 2143 2149 2160 rBV2 2658964 5675728 92.71% 17.903% 7 29.847 2697 2702 2709 rBV2 330879 654704 10.69% 2.065% 8 32.803 3017 3024 3045 rBV2 1789239 4275155 69.84% 13.485% 9 36.861 3459 3466 3485 rBV2 1176157 3216009 52.53% 10.144%

Sum of corrected areas: 31702007

31504.D GCMS0103.M Wed Feb 06 15:38:09 2002

NYC-WTC_000016630

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NYC-WTC_000016630Source: NYC Law Department, mirrored locally

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